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Volume 35 Issue 6
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Article Navigation >  Journal of Pharmaceutical Practice and Service  > 2017  >  35(6): 530-534

ZENG Lingjun, SONG Hongtao, FENG Yingli, CHENG Huihua. Quality control methods for Qihuang Fuzheng particle[J]. Journal of Pharmaceutical Practice and Service, 2017, 35(6): 530-534. doi: 10.3969/j.issn.1006-0111.2017.06.012
Citation: ZENG Lingjun, SONG Hongtao, FENG Yingli, CHENG Huihua. Quality control methods for Qihuang Fuzheng particle[J]. Journal of Pharmaceutical Practice and Service, 2017, 35(6): 530-534. doi: 10.3969/j.issn.1006-0111.2017.06.012
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Quality control methods for Qihuang Fuzheng particle

doi: 10.3969/j.issn.1006-0111.2017.06.012
  • 1.

    Department of Pharmacy, Fuzhou General Hospital, Fuzhou 350025, China

  • 2.

    Department of Radiation Oncology, Fuzhou General Hospital, Fuzhou 350025, China

  • Received Date: 2017-03-03
  • Rev Recd Date: 2017-06-30
  • Objective To establish the quality control methods for Qihuang Fuzheng particle. Methods Astragali Radix, Rehmanniae Radix Praeparata, Corni Fructus, Chuanxiong Rhizoma, Angelicae Sinensis Radix, Paeoniae Radix Rubra, Moutan Cortex, and Ophiopogonis Radix were identified with TLC. HPLC method was used for loganin assay in Corni Fructus. Results TLC identification methods for the main components were established. The TLC spots were clear with good separation. No interference was detected from the negative samples. The peak response and concentration of loganin showed good linear relationship over the range of 4.02-80.40 μg/ml (r=0.999 9). The mean recovery of loganin was 99.02%(RSD=0.64%, n=9). Conclusion The established quality control methods are accurate, reliable, and specific, which lay a foundation for the quality control of Qihuang Fuzheng particle.
  • [1] 曾令军,宋洪涛,陈惠华,等. 前列丹颗粒的质量控制方法研究[J]. 中国药师,2016,19(3):474-477.
    [2] 国家药典委员会. 中华人民共和国药典2015年版(四部)[S]. 北京:中国医药科技出版社,2015:57.
    [3] 李霞,贾晓斌,陈彦,等.妇康宝颗粒质量标准研究[J]. 时珍国医国药,2006,17(4):601-602
    [4] 唐勇琛,梁学政,吕建伟,等.益水生新饮颗粒的质量标准[J]. 中国药师,2014,17(5):737-740
    [5] 曾令军,宋洪涛,李蔚,等. 心脑通口服液质量标准提高研究[J]. 解放军药学学报,2016,32(5):417-419.
    [6] 童晓东,陈志军,杨水英,等.益视明目颗粒的质量标准研究[J].现代中药研究与实践,2016,30(1):42-45.
    [7] 江涛,雷健,邢茂,等.口炎清胶囊的质量控制和稳定性试验[J]. 中国药业,2014,23(11):17-20.
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Quality control methods for Qihuang Fuzheng particle

doi: 10.3969/j.issn.1006-0111.2017.06.012
  • 1. Department of Pharmacy, Fuzhou General Hospital, Fuzhou 350025, China
  • 2. Department of Radiation Oncology, Fuzhou General Hospital, Fuzhou 350025, China
  • Received Date: 2017-03-03
  • Rev Recd Date: 2017-06-30

Abstract: Objective To establish the quality control methods for Qihuang Fuzheng particle. Methods Astragali Radix, Rehmanniae Radix Praeparata, Corni Fructus, Chuanxiong Rhizoma, Angelicae Sinensis Radix, Paeoniae Radix Rubra, Moutan Cortex, and Ophiopogonis Radix were identified with TLC. HPLC method was used for loganin assay in Corni Fructus. Results TLC identification methods for the main components were established. The TLC spots were clear with good separation. No interference was detected from the negative samples. The peak response and concentration of loganin showed good linear relationship over the range of 4.02-80.40 μg/ml (r=0.999 9). The mean recovery of loganin was 99.02%(RSD=0.64%, n=9). Conclusion The established quality control methods are accurate, reliable, and specific, which lay a foundation for the quality control of Qihuang Fuzheng particle.

ZENG Lingjun, SONG Hongtao, FENG Yingli, CHENG Huihua. Quality control methods for Qihuang Fuzheng particle[J]. Journal of Pharmaceutical Practice and Service, 2017, 35(6): 530-534. doi: 10.3969/j.issn.1006-0111.2017.06.012
Citation: ZENG Lingjun, SONG Hongtao, FENG Yingli, CHENG Huihua. Quality control methods for Qihuang Fuzheng particle[J]. Journal of Pharmaceutical Practice and Service, 2017, 35(6): 530-534. doi: 10.3969/j.issn.1006-0111.2017.06.012
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