2003 Vol. 21, No. 6
Display Method:
2003, (6): 341-343.
Abstract:
OBJECTIVE To establish the method of assay for the bacterial endotoxin in papaverine hydrochlo-ride and sodium chloride injection. METHODS Inhibition and enhancement test was performed with limulus ameboeytc lysate manufactured by two different compa...
OBJECTIVE To establish the method of assay for the bacterial endotoxin in papaverine hydrochlo-ride and sodium chloride injection. METHODS Inhibition and enhancement test was performed with limulus ameboeytc lysate manufactured by two different compa...
2003, (6): 343-345.
Abstract:
OBJECTIVE To establish an HPLC method for the determination of zoledronic acid for injection. METHOD:The analysis was achieved by using Diamonsil C18 column with acetonitrile-ion-pair buffer solution(25:75)as mobile phase and UV-detector at wavelengt...
OBJECTIVE To establish an HPLC method for the determination of zoledronic acid for injection. METHOD:The analysis was achieved by using Diamonsil C18 column with acetonitrile-ion-pair buffer solution(25:75)as mobile phase and UV-detector at wavelengt...
2003, (6): 345-346.
Abstract:
OBJECTIVE To establish a HPLC method for the determination of Geniposide in Qingkailing Solution. METHODS The column Shimadzu ODS was used. The mobile phase was acetonitrile and water(15:85). The detection wavelength was 238nm. RESULTS:The average re...
OBJECTIVE To establish a HPLC method for the determination of Geniposide in Qingkailing Solution. METHODS The column Shimadzu ODS was used. The mobile phase was acetonitrile and water(15:85). The detection wavelength was 238nm. RESULTS:The average re...
2003, (6): 347-349.
Abstract:
OBJECTIVE To establish a new method to detect the two components of Psoralea corylifolia as a additive in cigarette and smoke. METHODS The SPME-GC-MS-SIM was used. RESULTS:The components(psoralen,isopsoralen)have been detected respectively. CONCLUSIO...
OBJECTIVE To establish a new method to detect the two components of Psoralea corylifolia as a additive in cigarette and smoke. METHODS The SPME-GC-MS-SIM was used. RESULTS:The components(psoralen,isopsoralen)have been detected respectively. CONCLUSIO...
2003, (6): 351-353.
Abstract:
OBJECTIVE An HPLC method was developed for determination of dl-Tetrahydropamatine in Yan-husuo. METHOD:The column was ODS Agilent zobax Extend C18(4.6×250mm,5μm),mobile phase was Meth-anol-0.1%. phosphoric acid(adjust pH 6.0 with Triethylamine)(55:45...
OBJECTIVE An HPLC method was developed for determination of dl-Tetrahydropamatine in Yan-husuo. METHOD:The column was ODS Agilent zobax Extend C18(4.6×250mm,5μm),mobile phase was Meth-anol-0.1%. phosphoric acid(adjust pH 6.0 with Triethylamine)(55:45...
2003, (6): 353-355.
Abstract:
OBJECTIVE To determine the content of ferulic acid in Fufang Danggui Diwan. METHODS HPLC was used. the mobile phase consisted of methanol - 1% glacial acetic acid(30:70). detection wavelengh was 323nm. RESULTS:The average recovery ratewas 98.90% with...
OBJECTIVE To determine the content of ferulic acid in Fufang Danggui Diwan. METHODS HPLC was used. the mobile phase consisted of methanol - 1% glacial acetic acid(30:70). detection wavelengh was 323nm. RESULTS:The average recovery ratewas 98.90% with...
2003, (6): 355-357.
Abstract:
OBJECTIVE To establish a GC method for the determination of organic solvents remaining. METHODS The methods was approved by high efficiency chlomatogram column of INNOWAX(30m×0.32mm×0.25μm),with a detector of FID using direct injection. RESULTS:There...
OBJECTIVE To establish a GC method for the determination of organic solvents remaining. METHODS The methods was approved by high efficiency chlomatogram column of INNOWAX(30m×0.32mm×0.25μm),with a detector of FID using direct injection. RESULTS:There...
2003, (6): 357-359.
Abstract:
OBJECTIVE To establish the fingerprint method for semen coicis. METHODS The Discovery® C18column with acetonitrile-ichloromethanol(59:41)as the mobile phase was used in HPLC-ELSD. The flow rate was 0.5mL/min and ELSD tube temperature is 70℃. The flow...
OBJECTIVE To establish the fingerprint method for semen coicis. METHODS The Discovery® C18column with acetonitrile-ichloromethanol(59:41)as the mobile phase was used in HPLC-ELSD. The flow rate was 0.5mL/min and ELSD tube temperature is 70℃. The flow...
2003, (6): 360-361.
Abstract:
OBJECTIVE To improve the judgement method of Chloragenic acid in Fufang Daqingye Heji. METHODS To change the eluant of ethyl acetate - methanol - water form(10:2:3)to(10:4:6)and change the turns by smoked the thin layer in ammonia first and then obse...
OBJECTIVE To improve the judgement method of Chloragenic acid in Fufang Daqingye Heji. METHODS To change the eluant of ethyl acetate - methanol - water form(10:2:3)to(10:4:6)and change the turns by smoked the thin layer in ammonia first and then obse...
2003, (6): 362-364.
Abstract:
OBJECTIVES:To establish the TLC method of Nubao capsules, and ensure the safety and effect of clinical application. METHODS Flos Carthami, Radix Angelicae Sinensls, Rhizoma Chuanxiong, Radix Paeoniae Alba, Pericarpium Citri Reticulutae were identifie...
OBJECTIVES:To establish the TLC method of Nubao capsules, and ensure the safety and effect of clinical application. METHODS Flos Carthami, Radix Angelicae Sinensls, Rhizoma Chuanxiong, Radix Paeoniae Alba, Pericarpium Citri Reticulutae were identifie...
2003, (6): 367-369.
Abstract:
OBJECTIVE Promethazine Hydrocloride and Chlordiazepoxide were determined by HPLC in Fu-fang Luotuma Pian I. METHODS Phenomenex - ODS3 Column(250×4. 60mm,5μm),the mobile phase consisted of a mixtur mixture of methanol-phosphate buffer(dissolved 2.64g ...
OBJECTIVE Promethazine Hydrocloride and Chlordiazepoxide were determined by HPLC in Fu-fang Luotuma Pian I. METHODS Phenomenex - ODS3 Column(250×4. 60mm,5μm),the mobile phase consisted of a mixtur mixture of methanol-phosphate buffer(dissolved 2.64g ...
2003, (6): 369-370.
Abstract:
OBJECTIVE To develop a method for the determination of ephedrine hydrochloride in kegan nasal drops by HPLC. METHODS The chromatographic condition included ODS column and the mobile phase consisting of 0.01 mol/L KH2PO4 solution-acetonitrile(40:60).T...
OBJECTIVE To develop a method for the determination of ephedrine hydrochloride in kegan nasal drops by HPLC. METHODS The chromatographic condition included ODS column and the mobile phase consisting of 0.01 mol/L KH2PO4 solution-acetonitrile(40:60).T...
2003, (6): 371-373.
Abstract:
OBJECTIVE Dissolution of sibutramine hydrochloride tablet was determinated by HPLC. The chromatography conditions were as follows:Column, Shimadzu VP-ODS; mobile phase:methol -0.05mol/L KH2PO4(adjusted to pH 3.0 with H3P04)(70:30);velocity of flow:1m...
OBJECTIVE Dissolution of sibutramine hydrochloride tablet was determinated by HPLC. The chromatography conditions were as follows:Column, Shimadzu VP-ODS; mobile phase:methol -0.05mol/L KH2PO4(adjusted to pH 3.0 with H3P04)(70:30);velocity of flow:1m...
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